Date of Award
1-1-2000
Thesis Type
Masters
Document Type
Thesis
Divisions
Faculty of Science
Department
Department of Chemistry
Institution
Universiti Malaya
Abstract
A preliminary work involving method development for normal stationary phase (silica) pennits the high-performance liquid chromatographic separation or aliphatic and polyaromatic hydrocarbon (PAHs) classes. The Soxhlet extraction method was applied on the coal rock samples and normal phase (silica) short column clean-up separation from highly polymeric material in the coal extract. Method developed on analytical and preparative normal phase silica HPLC columns were to fractionate coal rock extracts, isocratic elution of hexane: ethyl acetate (95 :5, V:V) was found to be quite a good mobile phase. An alternative fractionation method, preparative thin layer chromatography (TLC), was also investigated to separate the various organic groups in the organic extract from coal rocks from Batu Arang, Selangor.
Additional Information
Dissertation (M.A) -- Faculty of Science, Universiti Malaya, 2000.
Recommended Citation
Audrey, Yong Chee Hui, "Method development by HPLC for separation of various hydrocarbon groups in coal samples from Batu Arang, Selangor" (2000). Student Works (2000-2009). 167.
https://knova.um.edu.my/student_works_2000s/167
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