Amine functionalized magnetic nano-composite materials for the removal of selected endocrine disrupting compounds and its mechanism study

Document Type

Article

Publication Date

8-1-2020

Abstract

A novel adsorbent successfully synthesized using recyclable silica, nano magnetite and N1-(3 trimethoxisilylpropyl) diethylenetriamine (TRIS) denoted as MNCMT. Three endocrine disrupting compounds (EDCs) such as bisphenol A (BPA), ibuprofen (IBP) and clorofibric acid (CFA) were selected as model drugs for this study. The sorption capacities of EDCs by MNCMT were found to be 182.6 mg g(-1) for BPA, followed by CFA at 101.8 mg g(-1) and 72.6 mg g(-1) for IBP. The removal process matched with Langmuir isotherm and pseudo second order kinetic models with determination coefficient (R-2) above 0.99. The adsorbent was regenerated, recovered and reused for multiple cycles of adsorption. The physical-chemical properties and experimental data revealed that the chemical sorption is more dominant than physical sorption. Hydrogen bonding, pi-pi and electrostatic attractions provide intrinsic information on the removal mechanism.

Keywords

Magnetic adsorbent, EDCs, TRIS coated, Isotherm, Kinetic, Mechanism

Publication Title

Journal of Environmental Chemical Engineering

Divisions

ocean

Funders

Universiti Malaya (Grant No. RP 19A-13AET, RP008C-14SUS, RU 0030-2017)

Volume

8

Issue

4

Publisher

Elsevier Sci Ltd

Publisher Location

THE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLAND

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