Di-cationic Ionic Liquid Catalyzed Synthesis of 1,5-Benzothiazepines

Document Type

Article

Publication Date

1-1-2017

Abstract

A simple and elegant method for the synthesis of 1,5-benzothiazepines has been developed using di-cationic liquid as a solvent cum catalyst by the reaction of o-aminothiophenol with a variety of chalcones under mild reaction conditions. Furthermore the reusability of the catalyst has also been studied for three cycles. All the reactions are proposed to proceed through a 1,4-conjugate Michael addition followed by a cyclo-condensation reaction.

Keywords

gem-Dicationic ionic liquids, 1, 5-Benzothiazepines, 1, 5-Benzodiazepines, Cyclo-condensation reaction, Reusability

Divisions

CHEMISTRY,GEOLOGY

Funders

University of Malaya: research fellowships,Malaysian Ministry of Science, Technology and Innovation (MOSTI) through IPharm for the grant No. 53-02-03-1059

Publication Title

Asian Journal of Chemistry

Volume

30

Issue

1

Publisher

Chemic Publishing Company

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