Document Type

Article

Publication Date

1-1-2012

Abstract

In the thio­carbonohydrazide mol­ecule of the title compound, C17H12N6O2S·C4H8O, the terminal indolin-2-one ring systems make a dihedral angle of 20.13 (6)° with each other. Two intra­molecular N—H⋯O hydrogen bonds are present, each of which generates an S(6) ring. In the crystal, N—H⋯O hydrogen bonds lead to a mol­ecular chain running along the b axis. The tetra­hydro­furan solvent mol­ecule is disordered over two orientations in a 0.561 (11):0.439 (11) ratio.

Keywords

single-crystal X-ray study, T = 296 K, mean σ(C–C) = 0.002 A°, disorder in solvent or counterion, R factor = 0.040, wR factor = 0.121, data-toparameter ratio = 13.2.

Divisions

CHEMISTRY

Publication Title

Acta Crystallographica Section E: Structure Reports Online

Volume

68

Issue

Pt. 6

Publisher

International Union of Crystallography

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