1,3-Bis{[(4-methylphenyl)sulfonyl]-oxy}propan-2-yl 4-methylbenzene-sulfonate
Document Type
Article
Publication Date
1-1-2012
Abstract
In the title sulfonate derivative,C 24H 26O 9S 3, all atoms apart from those of one of the 4-methyl-benzene-sulfonate residues lie approximately in a disc; the dihedral angles between the approximately orthogonal benzene ring and those in the plane are 74.53 (9) and 67.79 (11)°. In the crystal, molecules are consolidated into the three-dimensional architecture by C - H⋯O interactions. One of the 4-methyl-benzene-sulfonate residues is disordered over two almost parallel positions; the major component refined to a site-occupancy factor of 0.918 (2).
Keywords
Data-to-parameter ratio = 14.3, Disorder in main residue, Mean σ(C-C) = 0.003 Å R factor = 0.035, single-crystal X-ray study, T = 100 K, wR factor = 0.100
Divisions
CHEMISTRY
Publication Title
Acta Crystallographica Section E: Structure Reports Online
Volume
68
Issue
3
Publisher
International Union of Crystallography
Additional Information
Department of Chemistry, Faculty of Science Building, University of Malaya, 50603 Kuala Lumpur, MALAYSIA