2-Chloro-N-[N-(4-chlorobenzoyl)hydrazinocarbothioyl]benzamide

Document Type

Article

Publication Date

1-1-2004

Abstract

The title compound, C15H11Cl2N 3O2S, has a similar structure and similar structural dimensions to the unsubstituted N-(N-benzoylhydrazinocarbothioyl)benzamide. However, the presence of Cl atoms at the para and ortho positions in the benzamide and benzoyl groups, respectively, caused the dihedral angle between these groups to increase from 16.42 (14)° in the unsubstituted compound to 74.96 (8)°. The molecule is stabilized by intermolecular C-H⋯O and N-H⋯S interactions, forming polymeric chains parallel to the c axis. © 2004 International Union of Crystallography Printed in Great Britain - all rights reserved.

Keywords

Acetone, Complexation, Crystal structure, Crystallization, Hydrazine, Hydrogen bonds, Isomers, Molecular dynamics, Molecular structure, Precipitation (chemical), Substitution reactions, X ray analysis, Atom numbers, Displacement ellipsoids, Intermolecular hydrogen bonds, Thiourea, Benzene

Divisions

CHEMISTRY

Publication Title

Acta Crystallographica Section E: Structure Reports Online

Volume

60

Issue

9

Publisher

International Union of Crystallography

Additional Information

Department of Chemistry, Faculty of Science Building, University of Malaya, 50603 Kuala Lumpur, MALAYSIA

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